Course Objectives: The learners should be able to:
Apply principles of separation and isolation techniques in organic reactions. Analyze NMR, IR and Mass spectra of organic compounds
Learning Outcomes: At the end of the course, the learners should be able to:
Separate and purify products in organic reactions
Characterize organic compounds using spectroscopic and spectrometric techniques
Course Contents:
Separation of two-component mixtures of organic compounds. Synthesis and isolation of organic compounds with an emphasis on different techniques of reaction set-up (air-sensitive, moisture-sensitive etc.), separation/purification (extraction, Soxhlet extraction, recrystallization, distillation, column chromatography) and monitoring of reaction by TLC, Structure determination of the isolated pure compounds by NMR spectroscopy, IR Spectroscopy and Mass spectrometry.
Text Books:
In-House laboratory manual with the experimental procedures and relevant literature.